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A Giant Molecular Spoked Wheel Article Options
Robert May, Stefan-S. Jester*, and Sigurd Höger* Kekulé-Institut für Organische Chemie und Biochemie, Rheinische Friedrich-Wilhelms-Universität Bonn, Gerhard-DomagkStrasse 1, 53121 Bonn, Germany
Cite this: J. Am. Chem. Soc. 136, 48, 16732-16735
J. Am. Chem. Soc., 2014, 136 (48), pp 16732–16735 DOI: 10.1021/ja5096705 Publication Date (Web): November 17, 2014 Copyright © 2014 American Chemical Society
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The modular synthesis of a defined, rigid molecular spoked wheel structure with the sum formula C1878H2682 and a diameter of about 12 nm is described. The attached 96 dodecyl side
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chains provide the solubility of the 25260 Da compound in common organic solvents. At the
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octanoic acid/highly oriented pyrolytic graphite interface, the molecules self-assemble to form an ordered 2D lattice, which is investigated by scanning tunneling microscopy, displaying their
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structure with submolecular resolution.
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Received 18 September 2014 Published online 17 November 2014 Published in print 3 December 2014
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