ANALYTICALß' BIOANALYTICAL CHEMISTRY [PDF]

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ANALYTICALß' BIOANALYTICAL CHEMISTRY Addresses of Editor

S. Daunert P. Garrigues G. Gauglitz K. G. Heumann K. Jinno A. Roda A. Sanz-Medel S. A. Wise

Sylvia Daunert Dept. Chemistry & Dept. Pharmaceutical Sciences University of Kentucky, Lexington, KY 40506-0055, USA Tel.: +1-859-257-7060,e-mail: [email protected] Philippe Garrigues Institut des Sciences Moléculaires (ISM), UMR 5255 CNRS Bâtiment A12. Université de Bordeauxl, 33405 Talence Cedex, France Tel.: +33-5-40006283,e-mail: [email protected]

Regional Editor Central Europe

M. Jarosz Central Editorial Office

Springer Tiergartenstrasse 17 69121 Heidelberg, Germany Managing Editor Christina Dyllick Associate Editor Andrea Pfeifer Assistant Editor Ingrid März Editorial Assistants Maite Menés Patricia Vogt Tel.: +49-6221-4878377 Fax: +49-6221-48768377 e-mail: [email protected] * The 'Instructions for Authors' can be found on the journal's website at www.springer.com/abc Authors are requested to submit their articles online. Please log directly onto the site http://mc.manuscriptcentral.com/abc and upload your manuscripts following the instructions given on the screen.

Günter Gauglitz Inst. Physikalische & Theoretische Chemie, Universität Tübingen Auf der Morgenstelle 8,72076 Tübingen, Germany Tel.: +49-7071-29-76927 or -74667, e-mail: [email protected] Klaus G. Heumann Inst. Anorg. Chemie & Analytische Chemie, Johannes Gutenberg-Universität Duesbergweg 10-14, 55099 Mainz, Germany Tel.: +49-6131-39-25882, e-mail: [email protected] Kiyokatsu Jinno School of Materials Science, Toyohashi University of Technology Toyohashi 441-8580,Japan Tel.: +81-532-446805, e-mail: jinnoSchrom.tutms.tut.ac.jp Aldo Roda Laboratory of Analytical and Bioanalytical Chemistry Dept. of Pharmaceutical, Sciences, Alma Mater Studiorum-University of Bologna, Via Belmeloro 6,40126 Bologna, Italy Tel. and Fax: +39-051-343398, e-mail: [email protected] Alfredo Sanz-Medel Dept. Physical & Analytical Chemistry, University of Oviedo CI Julián Claveria 8, 33 006 Oviedo, Spain Tel.: +34-985-103474, e-mail: [email protected] Stephen A. Wise National Inst. of Standards & Technology 100 Bureau Drive, Stop 8390, Gaithersburg, MD 20899-8390, USA Tel.: +1-301-975-3108, e-mail: [email protected] Address of Regional Editor

Maciej Jarosz Faculty of Chemistry Warsaw University of Technology Noakowskiego 3 00-664 Warsaw, Poland Tel. and Fax: +48-22-234-7408, e-mail: [email protected]

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ANALYTICALcSr BIOANALYTICAL CHEMISTRY Volume 397 Number 1 May 2010 ANALYTICAL CHALLENGE Avogadro constant challenge W.B. Jensen • J. Meija 1 Solution to the beryllium valence challenge J. Meija 3

Euroanalysis XV The European Conference on Analytical Chemistry Guest Editors: Wolfgang Buchberger • Wolfgang Lindner EDITORIAL Euroanalysis XV, 2009: The European conference on analytical chemistry W. Buchberger • W. Lindner 5 ABCS OF TEACHING ANALYTICAL SCIENCE E-learning in applied instrumental analysis: the example of cultural heritage preservation E.A. Varella 7 FEATURE ARTICLE Some people and places important in the history of analytical chemistry in Austria D.T. Burns 11

Application of the novel 5-chloro-2,2,3,3,4,4,5,5octafluoro-1-pentyl chloroformate derivatizing agent for the direct determination of highly polar water disinfection byproducts M. Vincenti • F. Fasano • M.C. Valsania • P. Guarda • S.D. Richardson 43 ORIGINAL PAPERS Food Analysis An inimunochemical test for rapid screening of zearalenone and T-2 toxin E.Y. Basova • I.Y. Goryacheva • T.Y. Rusanova • N.A. Burmistrova • R. Dietrich • E. Märtlbauer • C. Detavernier • C. Van Peteghem • S. De Saeger 55 Direct chiral determination of free amino acid enantiomers by two-dimensional liquid chromatography: application to control transformations in E-beam irradiated foodstuffs V. Guillén-Casla • M.E. León-González • L.V. Pérez-Arribas • L.M. Polo-Diez 63 Exploiting automatic on-line renewable molecularly imprinted solid-phase extraction in lab-on-valve format as front end to liquid chromatography: application to the determination of riboflavin in foodstuffs H.M. Oliveira • M.A. Segundo • J.L.F.C. Lima • M. Miró • V. Cerdà 77 Determination of aflatoxin Bj in alcoholic beverages: comparison of one- and two-photon-induced fluorescence C. Rasch • M. Böttcher • M. Kumke 87

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PAPERS IN FOREFRONT

Development and validation of a LC-MS/MS method for the simultaneous determination of aflatoxins, dyes and pesticides in spices C. Ferrer Amate • H. Unterluggauer • R.J. Fischer • A.R. Fernández-Alba • S. Masseiter 93

The principle of exhaustiveness versus the principle of parsimony: a new approach for the identification of biomarkers from proteomic spot volume datasets based on principal component analysis E. Marengo • E. Robotti • M. Bobba • F. Gosetti 25

Fluctuation in the ergosterol and deoxynivalenol content in barley and malt during malting process V. Dohnal • A. Jezkova • L. Pavlikova • K. Musilek • D. Jun • K. Kuca 109

The environmental challenge for analytical sciences M. Grasserbauer 17

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ANALYTICAL BIOANALYTICAL CHEMISTRY Comparison of two derivatization-based methods for solid-phase microextraction-gas chromatography-mass spectrometric determination of bisphenol A, bisphenol S and biphenol migrated from food cans P. Viñas • N. Campillo • N. Martinez-Castillo • M. Hernández-Córdoba 115 Validated HPAEC-PAD method for prebiotics determination in synbiotic fermented milks during shelf life C. Borromei • A. Cavazza • C. Corradini • C. Vatteroni • A. Bazzini • R. Ferrari • P. Menisi 127

Pharmaceutical Analysis Identification of a new co-crystal of salicylic acid and benzamide of pharmaceutical relevance M.A. Elbagerma • H.G.M. Edwards • T. Munshi • IJ. Scowen 137 Quantitative LC-ESI-MS/MS metabolic profiling method for fatty acids and lipophilic metabolites in fermentation broths from ß-lactam antibiotics production S. Schiesel • M. Lämmerhofer • W. Lindner 147 Development of an LC-MS/MS method for analysis of interconvertible Z/E isomers of the novel anticancer agent, Bp4eT J. Stariat • P. Kovaríková • J. Klimes • D.S. Kalinowski • D.R. Richardson 161 Determination of adrenolytic drugs by SPME-LC-MS B. Buszewski • P. Olszowy • T. Ligor • M. Szultka • J. Nowaczyk • M. Jaworski • M. Jackowski 173 Quantification of chlorpheniramine maléate enantiomers by ultraviolet spectroscopy and chemometric methods P. Valderrama • A.L. Romero • P.M. Imamura • I.R.S. MagaMes • P.S. Bonato • R.J. Poppi 181 Electrochemical evaluation and determination of antiretroviral drug fosamprenavir using boron-doped diamond and glassy carbon electrodes M. Gumustas • S.A. Ozkan 189 Biological Analysis Determination of insoluble avian eggshell matrix proteins I. Miksik • P. Sedláková • K. Lacinová • S. Pataridis • A. Eckhardt 205

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Raman spectroscopic analysis of minerals and organic molecules of relevance to astrobiology A.I. Alajtal • H.G.M. Edwards • I.J. Scowen 215 Determination of heterocyclic amines in urine samples by capillary liquid chromatography with evaporated light-scattering detection F. De Andrés • M. Zougagh • G. Castañeda • A. Ríos 223 Voltammetric detection of damage to DNA caused by nitro derivatives of fluorene using an electrochemical DNA biosensor V. Vyskocil • J. Labuda • J. Barek 233 Environmental Analysis Simultaneous determination by ultra-performance liquid chromatography-atmospheric pressure chemical ionization time-of-flight mass spectrometry of nitrated and oxygenated PAHs found in air and soot particles G. Mirivel • V. Riffault • J.-C. Galloo 243 Determination of brominated diphenyl ethers (from mono- to hexa- congeners) in indoor dust by pressurised liquid extraction with in-cell clean-up and gas chromatography-mass spectrometry M.P. Martinez • J.D. Carrillo • M.T. Tena 257 Determination of organic UVfiltersin water by stir bar sorptive extraction and direct analysis in real-time mass spectrometry M. Haunschmidt • C.W. Klampfl • W. Buchberger • R. Hertsens 269 Method for the simultaneous determination of the most problematic families of organic pollutants in compost and compost-amended soil M.M. González • J.L. Santos • I. Aparicio • E. Alonso 277 Holistic visualisation of the multimodal transport and fate of twelve Pharmaceuticals in biosolid enriched topsoils L. Barron • E. Nesterenko • K. Hart • E. Power • B. Quinn • B. Kelleher • B. Pauli 287 Capillary liquid chromatography with off-line mid-IR and Raman micro-spectroscopic detection: analysis of chlorinated pesticides at ppb levels S. Armenta • B. Lendl 297 GC-MS determination of polycyclic aromatic hydrocarbons evolved from pyrolysis of biomass D. Fabbri • A. Adamiano • C. Torri 309

Miscellaneous Multimethod analysis of Iranian Ilkhanate ceramics from the Takht-e Soleyman palace L. Osete-Cortina • M.T. Doménech-Carbó • A. Doménech • DJ. Yusá-Marco • H. Ahmadi 319 Screen-printed sensor for batch and flow injection potentiometric chromium(VI) monitoring R.A. Sánchez-Moreno • MJ. Gismera • M.T. Sevilla • J.R. Procopio 331

Determination of vanadium(V) in the particulate matter of emissions and working areas by sequential dissolution and solid-phase extraction M. Sturini • F. Maraschi • L. Cucca • G. Spini • G. Talamini • A. Profumo 395 Ultra-fast HPLC-ICP-MS analysis of oxaliplatin in patient urine G. Koellensperger • S. Hann 401

Investigation of selective molecular interactions using two-dimensional Fourier transform IR spectroscopy X. Liu • T. Zhou • X. Wang • J. Zhang

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Characterisation of steroids in wooden crates of veal calves by accelerated solvent extraction (ASE®) and ultra-high performance liquid chromatography coupled to triple quadrupole mass spectrometry (U-HPLC-QqQ-MS-MS) K. Verheyden • H. Noppe • J. Vanden Bussche • K. Wille • K. Bekaert • L. De Boever • J. Van Acker • C.R. Janssen • H.F. De Brabander • L. Vanhaecke 345 Identification of additives in poly(vinylacetate) artist's paints using PY-GC-MS M.F. Silva • M.T. Doménech-Carbó • L. Fuster-López • M.F. Mecklenburg • S. Martin-Rey 357 Volatile organic compounds in paper—an approach for identification of markers in aged books E.M. Gaspar • J.C. Santana • J.F. Lopes • M.B. Diniz 369 CMOS arrays as chemiluminescence detectors on microfluidic devices E.R.G.O. Rodrigues • R.A.S. Lapa 381 TECHNICAL NOTES Application of the new electroanalytical technique AGNES for the determination of free Zn concentration in river water F. Zavarise • E. Companys • J. Galceran • G. Alberti • A. Profumo 389

Indexed in/abstracted by Current Contents, Science Citation Index, Analytical Abstracts, Chemical Abstracts, BIOSIS, Aquatic Sciences and Fisheries Abstracts, Food Science and Technology Abstracts, Life Science Collection, Pascal, Index Medicus and Mediine Instructions for Authors for Anal Bioanal Chem are available at http^/www.springer.com/abc Cover image: SEM backscattered electron image of the metallic sheet fixed on the glaze of the sample CI7VC (reference 20986-10). Metallic sheet on the top, and glaze at the bottom. (From L. Osete-Cortina, M.T. Doménech-Carbó, A. Doménech, DJ. Yusá-Marco, H. Ahmadi 'Multi-method analysis of Iranian Ilkhanate ceramics from the Takht-e Soleyman palace'. Anal Bioanal Chem (2010) 397: 319-329)

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