Eugene Kapustin Degrees Aug-2014 - Omar Yaghi - UC Berkeley [PDF]

Degrees. Aug-2014 – present. Ph.D. in chemistry, UC Berkeley, USA. • Advisor: Prof. Omar M. Yaghi. Sep-2013 – pres

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Eugene A. Kapustin 32 Lewis Hall, University of California-Berkeley, Berkeley, CA 94720 phone: 513.680.1513 [email protected] orcid.org/0000-0003-4095-9729

Education Ph.D. in Chemistry, University of California-Berkeley, USA Advisor: Prof. Omar M. Yaghi Thesis: Structure of guests in MOF and their applications

08/2014 – 05/2018

Ph.D. in Chemistry, Novosibirsk State University, Russia Advisor: Prof. Elena V. Boldyreva Thesis: The role of intermolecular interactions in N-methylated derivatives of glycine in the formation of crystalline structures

09/2013 – 02/2016

Diploma in Chemistry, Novosibirsk State University, Russia

09/2008 – 06/2013

Research Experience Graduate Student Researcher in Prof. Yaghi’s Group University of California-Berkeley, Lawrence Berkeley National Lab Structural and sorption studies of crystalline extended porous materials, including coordinative alignment (CAL) method and water harvesting from desert air using metal-organic frameworks (MOFs)

08/2014 – present

Graduate Student Researcher in Prof. Boldyreva’s Group Institute of Solid State Chemistry and Mechanochemistry SB RAS Study of the influence of intermolecular interactions on the distortion of crystal structures under external loads and their rearrangements during phase transitions

09/2012 – 07/2014

Visiting Undergraduate Student in Prof. Boulatov’s Group University of Illinois at Urbana-Champaign Investigation of the kinetics of the hydrolysis of esters under restoring mechanical force using stiff stilbene as molecular force probes

01/2012 – 08/2012 07/2011 – 09/2011

Visiting Undergraduate Student in Prof. Schaefer’s Group University of Cincinnati Study of corrosion protection and surface treatment for aluminum alloys using chromate-free technology

06/2010 – 09/2010

2 | Curriculum vitae Eugene A. Kapustin Technical Expertise 6+ years of experience in the field of single-crystal X-ray crystallography: a) Structural characterization of molecular crystals and MOFs at ambient conditions b) Investigation of structural rearrangements in amino acids during phase transitions c) Crystallography using the CAL method d) High-pressure crystallography in diamond-anvil cells e) Study of single-crystalline covalent organic frameworks f) User of ALS and SSLS synchrotron facilities 4+ years of experience in the field of gas and vapor sorption: a) Low- and high-pressure gas sorption measurements with MOFs and COFs b) Sorption kinetics measurement with MOFs and their performance evaluation c) Design and fabrication of MOF-based water harvesting devices Mastery in the operation and maintenance of sorption and X-ray diffraction instruments Proficiency in the arsenal of characterization techniques for solids: a) Powder X-ray diffraction analysis b) Powder neutron diffraction analysis c) Optical and scanning electron microscopy d) UV-vis, IR and near-IR spectropscopy e) Thermogravimetry and differential scanning calorimetry f) ICP mass spectrometry Characterization of crystalline molecular fragments with polarized Raman spectroscopy Scaled-up synthesis and activation of MOFs for water harvesting purposes Application of spectroscopy and chromatography for the study of force-dependent kinetics Professional Activity Invited reviewer for Z. Kristallogr., Joule, ACS Appl. Mater. Interfaces. Technical reviewer for Science, J. Am. Chem. Soc., Angew. Chem. Int. Ed. Scientific collaborations with MIT, KACST, Peking & Lanzhou Universities, University of Liverpool Prepared the grant applications for NASA, ARPA-E, AFRL, DOE LDRD, KACST Teaching Experience Trained graduate students to perform gas sorption and X-ray diffraction experiments Supervised graduate students and post-doctoral researchers conducting gas sorption and X-ray diffraction experiments; analyzed the collected data and prepared for publication CHEM 105 – Instrumental Methods in Analytical Chemistry for Undergraduates (Spring 2017) CHEM 4B – General Chemistry and Quantitative Analysis for Undergraduates (Spring 2016) CHEM 1A – General Chemistry for Undergraduates (Fall 2014)

3 | Curriculum vitae Eugene A. Kapustin Publications 1. Ma, T.-Q.,# Kapustin, E. A.,# Yin, S. X., Liang, L., Zhou, Z., Niu, J., Li, L.-H., Wang, Y., He, G., Su, J., Li, J., Wang, X., Wang, W. D., Wang, W., Sun, J., Yaghi, O. M. Science 2018 361, 48– 52. 2. Fathieh, F.,# Kalmuztki, M. J.,# Kapustin, E. A.,# Waller, P. J., Yang, J., Yaghi, O. M. Science Adv. 2018 4, eaat3198. 3. Hong, C. M.,# Morimoto, M.,# Kapustin, E. A., Alzakhem, N., Bergman, R. G., Raymond, K. N., Toste, F. D. J. Am. Chem. Soc. 2018 140, 6591–6595. 4. Kapustin, E. A. Chem 2018, 4, 16–27. 5. Kim, H.,# Rao, S.,# Kapustin, E. A., Zhao, L., Yang, S., Yaghi, O. M., Wang, E. N. Nature Commun. 2018 9, 1991. 6. Diercks, C. S.,# Lin, S.,# Kornienko, N., Kapustin, E. A., Nichols, E. M., Zhu, C., Zhao, Y., Chang, C. J., Yaghi, O. M. J. Am. Chem. Soc. 2018, 140, 1116–1122. 7. Kapustin, E. A., Lee, S., Alshammari, A. S., Yaghi, O. M. ACS Central Science 2017, 3, 662– 667. 8. Kim, H., Yang, S., Rao, S. R., Narayanan, S., Kapustin, E. A., Furukawa, H., Umans, A. S., Yaghi, O. M., Wang, E. N. Science 2017, 356, 430–434. 9. Flaig, R. W., Popp Osborn T. M., Fracaroli, A. M., Kapustin, E. A., Kalmutzki, M. J., Altamimi, R. M., Fathieh, F., Reimer, J. A., Yaghi, O. M. J. Am. Chem. Soc. 2017, 139, 12125–12128. 10. Zhao, Y.,# Guo, L.,# Gándara, F., Ma, Y., Liu, Z., Zhu, C., Lyu, H., Trickett, C. A., Kapustin, E. A., Terasaki, O., Yaghi, O. M. J. Am. Chem. Soc. 2017, 139, 13166–13172. 11. Lee, S., Kapustin, E. A., Yaghi, O. M. Science 2016, 353, 808–811. 12. Kapustin, E. A., Minkov, V. S., Boldyreva, E. V. PCCP 2015, 17, 3534–3543. 13. Kapustin, E. A., Minkov, V. S., Stare, J., Boldyreva, E. V. Cryst. Growth Des. 2014, 14, 1851–1864. 14. Kapustin, E. A., Minkov, V. S., Boldyreva, E. V. Acta Cryst. B 2014, 70, 517–532. 15. Kapustin, E. A., Minkov, V. S., Boldyreva, E. V. CrystEngComm 2014, 16,10165–10168. 16. Akbulatov, S., Tian, Y., Kapustin, E., Boulatov, R. Angew. Chem. Int. Ed. 2013, 52, 6992– 6995. 17. Minkov, V. S., Kapustin, E. A., Boldyreva, E. V. Acta Cryst. C 2013, 69, 416–420. Presentations and Conferences 1. E. A. Kapustin. “Coordinative Alignment Method for Crystallographic Study of Gas Sorption”, CGS Nanoporous Seminar, Berkeley, USA, October 25, 2017 – Oral. 2. E. Kapustin. “Metal-Organic Frameworks for Drinking Water”, CellPress Lablinks Meeting, Berkeley, USA, September, 18, 2017 – Oral.

4 | Curriculum vitae Eugene A. Kapustin 3. E. A. Kapustin, S. Lee, O. M. Yaghi. “Coordinative alignment of molecules in chiral metalorganic framework”, 24th Congress and General Assembly of the International Union of Crystallography, Hyderabad, India, August, 21-28, 2017, Acta Cryst. (2017). A73, C794 – Oral. 4. E. A. Kapustin, S. Lee, O. M. Yaghi. “Molecular retrofitting adapts a metal-organic framework to extreme pressure”, 2016 All-Hands CGS Meeting, Berkeley, USA, November 8-9, 2016 – Oral. 5. E. Kapustin, V. Minkov, E. Boldyreva. “Sarcosine and betaine crystals on cooling – structural motifs unstable at high pressure become stable at low temperatures”, Deutsche Gesellschaft für Kristallographie, 23. Jahrestagung, Berlin, Germany, March 1619, 2015. P01 – Poster. 6. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva “Effect of pressure on methylated glycine derivatives: relative roles of hydrogen bonds and steric repulsion of methyl groups”, 52nd EHPRG Meeting on High Pressure Science and Technology, Lyon, France, September 7-12, 2014. P01 – Poster. 7. E. Kapustin, V. Minkov, E. Boldyreva. “The Only N-H···O Hydrogen Bond - Two Ways to Build a Structure of Dimethylglycine”, 23rd Congress and General Assembly of the International Union of Crystallography, Montreal, Canada, August 5-12, 2014. Acta Cryst. (2014), A70, C550. – Poster. 8. E. Kapustin, V. Minkov, E. Boldyreva. “Effect of high pressure on the crystal structures of sarcosine and betaine”, 23rd Congress and General Assembly of the International Union of Crystallography, Montreal, Canada, August 5-12, 2014. Acta Cryst. (2014), A70, C272. – Poster. 9. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva. “Pressure induced phase transitions in glycine derivatives sarcosine and betaine: relative roles of H-bonds, steric repulsion of methyl-groups, and dipole-dipole interactions”, International Symposium on the Reactivity of Solids (ISRS-18), St. Petersburg, Russia, June 9-13, 2014, P. 273 – Poster. 10. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva. “One hydrogen bond - two ways to build a structure. The role of N-H···O hydrogen bonds in crystal structures of N,Ndimethylglycine”, International Symposium on the Reactivity of Solids (ISRS-18), St. Petersburg, Russia, June 9-13, 2014, P. 274 – Poster. 11. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva. “Crystalline N-methylated glycines and investigation of low-temperature and high-pressure effects on their structures”, Annual Conference ISSCM SB RAS, Novosibirsk, Russia, May 28-29, 2014 – Oral. 12. E. Kapustin, V. Minkov, E. Boldyreva. “The only hydrogen bond - two ways to build a structure. The role of N-H···O hydrogen bond in crystal structures of N,Ndimethylglycine”, Deutsche Gesellschaft für Kristallographie, 22. Jahrestagung, Berlin, Germany, March 17-20, 2014, P. 84 – Poster.

5 | Curriculum vitae Eugene A. Kapustin 13. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva. “Effect of low temperatures on the crystal structures of N-methylated glycines”, 28th European Crystallographic Meeting, Warwick, UK, August 25-29, 2013, Acta Cryst. (2013). A69, s606 – Poster. 14. E. A. Kapustin, V. S. Minkov, E. V. Boldyreva. “Betaine 0.77-perhydrate 0.23-hydrate and common structural motifs in crystals of amino acids perhydrates”, 21st International Conference on the Chemistry of the Organic Solid State, Oxford, UK, August 5-9, 2013, P. 64 – Poster. 15. E. A. Kapustin, V. S. Minkov. “Crystalline N-methylated glycines and investigation of lowtemperature and high-pressure effects on their structures”, Abstracts of 51st International Student Scientific Conference, section of “Solid State chemistry”, Novosibirsk, Russia, April 12-16, 2013 – Oral. Media Coverage Interviews for Gizmodo “These (Real) New Moisture Harvesters Belong on Tatooine”; WIRED “Wanna Pull Water Out of Air? Grab Some Ions or a Weird Sponge”; Berkeley Lab News Center “A New Way to Display the 3-D Structure of Molecules”; Big Picture Science “Water from Air”; Catalyst Magazine “Wringing Drinking Water from Dry Air”; ABC News “Extracting drinking water from dry desert air is no longer a pipe dream”; UC Berkeley “In desert trials, nextgeneration water harvester delivers fresh water from air”; Smithsonian Magazine “This Device Pulls Water Out of Desert Air”; KCBS radio “Water from Air”; ATTN, Civil Engineering journal. Patent Applications 1. Yaghi, O. M., Lee, S., Kapustin, E. A., Coordinative Alignment of Molecules in MetalOrganic Frameworks for Structure Determination by Diffraction Techniques. Invention Disclosure submitted 2. Yaghi, O. M., Kapustin, E. A., Fathieh, F., Kalmutzki, M. J. Atmospheric Moisture Harvester. Invention Disclosure submitted References Omar M. Yaghi (Ph. D. advisor at University of California-Berkeley) [email protected] Elena V. Boldyreva (Ph. D. advisor at Novosibirsk State University) [email protected] Hans-Beat Bürgi (mentor and colleague) [email protected]

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